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Certified Reference Materials for Analytical quality control in Neutron Activation Analysis.

Wee, Boon Siong, and Abdul Khalik Hj. Wood, and Mohd. Suhaimi Hamzah, and Shamsiah Abdul Rahman, and Md. Suhaimi Elias, and Nazaratul Ashifa Abd. Salim , (2007) Certified Reference Materials for Analytical quality control in Neutron Activation Analysis. Malaysian Journal of Analytical Sciences, 11 (1). pp. 17-22. ISSN 13942506

Full text not available from this repository.

Official URL: http://pkukmweb.ukm.my/~mjas/v11_n1/03-063A6%20Edited%2025th%20June%202007-1.pdf

Affiliations

Malaysian Institute for Nuclear Technology Research

Abstract

Analytical quality control in neutron activation analysis (NAA) requires the use of certified reference materials (CRM) in order to produce reliable analytical results. It is essential to evaluate the performance of NAA method when analyzing various sample matrices. Therefore, the CRM selected for an analysis should be suitable for the type of samples. There are many aspects such as concentration range, matrix match, sample size, and uncertainty, which need to be considered when selecting a suitable CRM. Eventually, results of analysis of CRM were plotted into control charts in order to evaluate the quality of the data. This is to ensure that the results are within the 95% confidence interval as stipulated in the certificate of CRM. Thus, this article aims to discuss the uses of certified reference materials for quality control purposes in NAA involving various sample matrices.

Bahan rujukan piawai adalah berguna dalam kawalan mutu analisis dalam analisis pengaktifan neutron untuk memperolehi keputusan analisis yang boleh dipercayai. Ia juga penting dalam menilai keputusan kaedah NAA semasa menganalisa pelbagai bahan sampel. Oleh yang demikian, bahan rujukan piawai yang dipilih hendaklah bersesuaian dengan jenis sample yang dikaji. Terdapat beberapa factor yang perlu dipertimbangkan semasa memilih bahan rujukan piawai seperti julat kepekatan, kesesuaian matriks, saiz sampel, dan ketidakpastian. Keputusan analisis bahan rujukan piawai diplotkan dalam carta kawalan untuk menilai kualiti data. Ini adalah untuk memastikan keputsan adalah dalam lingkungan 95% confidence interval berbanding dengan sijik bahan rujukan piawai. Kertas kerja ini bertujuan untuk membincangkan kegunaan bahan rujukan piawai dalam kawalan mutu dalam analisis pengaktifan neutron yang melibatkan pelbagai jenis sampel.

Item Type:Journal
Keywords:Certified reference materials, analytical quality control, neutron activation analysis.
Subjects:Q Science
ID Code:997

1. ISO Guide 30 (1992). Terms and Definitions used in connection with reference materials, ISO, Geneva.

2. R. Walker and I. Lumley (1999). Pitfalls in terminology and use of reference materials. Trends Anal. Chem. 18, 594

– 616.

3. B. King (1997). Traceability of chemical analysis. Analyst 122, 197 – 204.

4. P. Bode and C.P. van Dijk (1997). Operational management of results in INAA utilizing a versatile system of control charts. J. Radioanal. Nucl. Chem. 215, 87 – 94.

5. Wee Boon Siong, H.M. Dung, Abdul Khalik Hj. Wood, Nazaratul Ashifa Abd. Salim and Muhamad Suhaimi Elias (2006). Testing the applicability of k0-INAA at the MINT’s TRIGA MK II reactor. Nucl. Instr. & Meth. A 564, 716 – 720.

6. M. Thompson (2000). Recent trends in inter-laboratory precision at ppb and sub-ppb concentrations in relation to fitness for purpose criteria in proficiency testing. Analyst 125, 385 – 386.

7. R. Zeisler, E.A. Mackey, G.P. Lamaze, T.E. Stover, R.O. Spatz and R.R. Greenberg (2006). NAA methods for determination of nanogram amounts of arsenic in biological samples. J. Radioanal. Nucl. Chem. 269, 291 – 296.

8. J. Kucera, P. Bode and V. Stepanek (2000). The 1993 ISO Guide to the expression of uncertainty in measurement applied to NAA. J. Radioanal. Nucl. Chem. 245, 115 – 122.

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